I-Lomefloxacin hydrochloride CAS 98079-52-8
Ubungozi Nokuphepha
| Izimpawu Eziyingozi | I-Xn - Iyingozi |
| Amakhodi Engozi | 22 – Kuyingozi uma kugwinywe |
| I-WGK Germany | 3 |
| I-RTECS | VB1997500 |
| Ikhodi ye-HS | 29339900 |
Ukuzimisela kokuqukethwe
Idatha Egunyaziwe Yedatha Eqinisekisiwe
kukalwa ngokusebenza okuphezulu kwechromatography ye-liquid (Okujwayelekile 0512).
izimo ze-chromatographic nokuhlolwa kokufaneleka kwesistimu
ijeli ye-silica ehlanganiswe ne-octylsilane njengesigcwalisi; Isixazululo se-sodium pentanesulfonate (i-sodium pentanesulfonate 1.5g, i-ammonium dihydrogen phosphate 3.0g, amanzi angu-950ml azoncibilika, lungisa i-pH ibe ne-phosphoric acid, nciphisa ibe ngu-1000ml ngamanzi) -Methanol (65:35) njengesigaba esihambayo, izinga lokugeleza elingu-1.2m iminithi, ubude begagasi bokutholwa obungu-287mn. Thatha isixazululo esisebenzayo sesistimu esingu-20u1 ngaphansi kwento yezinto ezihlobene futhi usijove ku-Liquid Chromatograph yomuntu. Isikhathi sokugcinwa kwe-lomefloxacin cishe imizuzu eyi-9, kanti izinga lokuhlukaniswa phakathi kwenani eliphakeme lokungcola ngesikhathi sokugcinwa okuhlobene cishe elingu-0.8 kanye nenani eliphakeme le-lomefloxacin kufanele libe likhulu kuno-2.0, ukulungiswa phakathi kwenani eliphakeme le-lomefloxacin kanye nenani eliphakeme lokungcola ngesikhathi sokugcinwa okuhlobene kufanele libe ngu-1.1. ukuhlangabezana nezidingo.
ukuhlola
thatha inani elilungile lalo mkhiqizo, isisindo esinembile, kanye nokuqedwa kwesigaba seselula kanye nokuhlanjululwa komthamo okwenziwe ku-lml ngayinye equkethe cishe u-0. Isixazululo se-lmg sisetshenziswe njengesixazululo sokuhlola, futhi u-20ul wajovwa ku-chromatograph ewuketshezi ngokunemba, kanye ne-chromatogram. yaqoshwa. Enye inkomba ye-lomefloxacin yathathwa futhi yanqunywa ngendlela efanayo. Okuqukethwe kwe-lomefloxacin (C17H19F2N303) kusampula kubalwe ngendawo ephakeme kakhulu ngokuya ngendlela evamile yangaphandle.
